Analytical 343

CHEM 3430:

Analytical Chemistry II

Winter 2004

Updated: 4/4/04

What's New:

· Quiz Outline for 1,2, and 3.

· Please be sure to READ the question on the exam. I strongly recommend reading the questions at least twice.

· I will be available April 5 to answer questions.

Calendar Description: Analytical Chemistry: Data Reduction, Chromatography, Spectroscopy, Electrochemistry

Course Instructor: Dr. Perry Martos, 767-6209 pmartos@lsd.uoguelph.ca

Lab Supervisor: Dr. Julie De Merchant extension 4861 jde@uoguelph.ca

Lectures: CM 260: Wednesday 7.00 - 10.00 PM

Office Hours: Office hours will be posted after the second week, but please contact me at any time when you need help.

Pre-Requisites 19-240 and 19-207

Labs: C&M 357

Lab Manual: Analytical Chemistry II: Instrumental Analysis CHEM*3430

Text: "Principles of Instrumental Analysis" Skoog, Holler, and Nieman. 5^th Edition (1998) (on reserve)

Evaluation:

Quizzes (6-8) 30%

Laboratory 30%

Final Exam 40% April 5, 2.30-4.30

Lecture Notes: Specific handouts will be provided throughout the course. Problem sets will be provided, in addition to solutions (as required). You will be responsible to download class notes.

Instructor Evaluation:

As part of the faculty evaluation process in the Department of Chemistry and Biochemistry, students are reminded that written comments on the teaching performance of the lecturer may be sent to the Chair, Department of Chemistry and Biochemistry, at any time. Such letters must be signed; a copy will be made available to the instructor after submission of final grades. You will also have the opportunity near the end of the course to evaluate me, the course, labs etc. through the evaluation forms.

Problem Sets

Problem Set 1

Problem Set 2

Problem Set 3 and Solutions

Problem Set 4 and Solutions

Problem Set 5

Course Notes:

Part One: Overview and Introduction

The first part of this course is intended to give you tools to effectively carry out data analysis.

· Overview and Introduction

· Terms and Definitions

· GLP: Good Laboratory Practices

· USP Information

Part Two: Sample Preparation, Chromatography and Detection

The focus of this part of the course is chromatography and sample preparation with SPE and SPME. These notes will be posted next week.

· Chromatography - general

· Chromatography - LC-MS/MS (in conjunction with Applied Biosystems)

I have also provided a set of slides on SPME and SPME2 (no longer required)

Part Three: Mass Spectrometry

The focus of this part of the course is on Mass Spectrometry. These notes will be posted early this week.

· Mass Spectrometry

Part Four: UV/VIS Spectroscopy

In this part of the course, we will look at the absorption of energy from photons, and the release of the absorbed energy as an analytical tool (fluorescence).

Spectroscopy (perspectives) Overview

Overview of Spectroscopy Part A

Overview of Spectroscopy Part B

Monochromators and Slits in Spectroscopy

Atomic Spectroscopy